Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Octanol → Propan-2-yl 2-dodecylbenzene-1-sulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Octanol | HCID 20083 | — |
| 반응물 | p-Toluenesulfonic acid 1-methylheptyl ester | HCID 3912199 | — |
| 반응물 | 2-Dodecylbenzene-1-sulfonyl chloride | HCID 20439001 | — |
| 생성물 | Propan-2-yl 2-dodecylbenzene-1-sulfonate | HCID 23368822 | 83% |
반응 단계
In the Example of preparation of material 18, 2-octanol was used in place of 2-propanol in the Example of preparation of material 17. In the Example of preparation of material 19, dodecylbenzene sulfonyl chloride was used in place of p-toluene sulfonyl chloride in the Example of preparation of material 17. Other procedures were made in the same way as the Example of preparation of material 17. In the Example of preparation of material 18, 1-methylheptyl p-toluene sulfonate was obtained in the yield of 72% and, in the Example of preparation of material 19, 1-methylethyl dodecylbenzene sulfonate was obtained in the yield of 83%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05319024 |
| 출처 데이터셋 | uspto-grants-1994_06 |
| ORD ID | ord-fcde6d5423e74d30ae06c643be62027b |
| 출처 메모 | uspto-grants-1994_06 |