Cesium fluoride → Allyl Oxalofluoride

HRID 1109259

반응식

HRID 1109259 반응식
[CH2:1]([O:4][C:5](=[O:9])[C:6](Cl)=[O:7])[CH:2]=[CH2:3].[F-:10].[Cs+]>>[CH2:1]([O:4][C:5](=[O:9])[C:6]([F:10])=[O:7])[CH:2]=[CH2:3]

참가 물질

3

반응물 2

HCID 25953Cesium fluorideHCID 3018516Allyl chlorooxoacetate

생성물 1

HCID 14153244Allyl Oxalofluoride

실험 절차

By the procedure of the preceding Preparation, allyl oxalochloride (252.5 g, 1.70 mol) and cesium fluoride (284 g, 1.87 mol) were converted to twice distilled title product, b.p. 48°-50° C./35 mm; 124°-126° C. (atmospheric pressure).

후처리

  1. distillationto twice distilled title product, b.p. 48°-50° C./35 mm
  2. custom124°-126° C. (atmospheric pressure)

출처 및 근거

ORD 기록
ord-f50bba0a23a44a65b38e743dc1911933
출처 데이터셋
uspto-grants-1994_06
특허 번호
US05319103

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