Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → 3-(6-Fluoroquinol-2-yl-trans-ethenyl)benzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Isophthalaldehyde | HCID 34777 | — |
| 반응물 | 6-Fluoro-2-methylquinoline | HCID 70784 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | 3-(6-Fluoroquinol-2-yl-trans-ethenyl)benzaldehyde | HCID 86747933 | 50.7% |
반응 단계
Using the procedure of Preparation I1, 5.04 g of 2-methyl-6-fluoroquinoline, 4.20 g of isophthaldehyde and 8.86 ml of acetic anhydride in 100 ml of xylene gave 4.40 g of the titled product as a pale yellow solid, m.p. 110°-111° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05322847 |
| 출처 데이터셋 | uspto-grants-1994_06 |
| ORD ID | ord-738497aa53d248f584e17253f2da180e |
| 출처 메모 | uspto-grants-1994_06 |