참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Carbon Dioxide | HCID 280 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | 2,6-Dichlorophenoxysulfonyl isocyanate | HCID 19018468 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 2,6-Dichlorophenyl sulfamate | HCID 19018467 | — |
반응 단계
2.6 ml of water are added dropwise at 30° C. to 40° C. to a solution of 24.4 g of 2,6-dichlorophenoxysulfonyl isocyanate in 200 ml of tetrachloromethane. The mixture is then stirred at room temperature until the evolution of carbon dioxide is complete and cooled to 0° C., the product is filtered off with suction and the residue is then washed with ice-cold tetrachloromethane. After drying in vacuo, 21.4 g of 2,6-dichlorophenyl sulfamate of melting point 108°-110° C. are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05324710 |
|---|
| 출처 데이터셋 | uspto-grants-1994_06 |
|---|
| ORD ID | ord-e54d7659cfb745089cd80515edce33e1 |
|---|
| 출처 메모 | uspto-grants-1994_06 |
|---|
