Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Isopropoxy-4-nitrotoluene → 4-Methyl-2-(propan-2-yloxy)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Isopropoxy-4-nitrotoluene | HCID 592731 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-Methyl-2-(propan-2-yloxy)aniline | HCID 15068114 | — |
반응 단계
5-Methyl-1-(1-methylethoxy)-2-nitrobenzene, 17.7 g (91 mmol), is dissolved in methanol, palladium on charcoal is added and the mixture is exposed to hydrogen gas until the required amount of hydrogen is absorbed. The mixture is worked up in the usual manner to give 15 g of 4-methyl-2-(1-methylethoxy)benzenamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04975456 |
| 출처 데이터셋 | uspto-grants-1990_12 |
| ORD ID | ord-7e4950a4355741209f6cd1b0394f8712 |
| 출처 메모 | uspto-grants-1990_12 |