Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Anthraquinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1-Amino-4-bromo-9,10-dihydro-9,10-dioxo-2-anthracenesulfonic acid | HCID 22628 | — |
| 반응물 | 4-(beta-Acetylaminoethylamino)aniline 3-sulfonic acid | HCID 22154633 | — |
| 생성물 | Anthraquinone | HCID 6780 | — |
반응 단계
1-Amino-4-bromoanthraquinone-2-sulfonic acid and 4-(β-acetylaminoethylamino)aniline 3-sulfonic acid were subjected to Ullmann condensation in the presence of cuprous chloride as a catalyst, followed by hydrolysis of the acetyl group under an acid condition of hydrochloric acid, thereby obtaining an anthraquinone intermediate compound of the following formula (2) in the free acid form ##STR493##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04977261 |
| 출처 데이터셋 | uspto-grants-1990_12 |
| ORD ID | ord-099f7899c2a749b4be25c544a68b049c |
| 출처 메모 | uspto-grants-1990_12 |