Vinyl Acetate → 1,1-Ethanediol, 1,1-diacetate

HRID 1111242

반응식

HRID 1111242 반응식
[C:1]([O:4][CH:5]=[CH2:6])(=[O:3])[CH3:2]>[Pd](Cl)Cl.C(O)(=O)C>[C:1]([O:4][CH:5]([O:4][C:1](=[O:3])[CH3:2])[CH3:6])(=[O:3])[CH3:2]

참가 물질

4

반응물 1

HCID 7904Vinyl Acetate

생성물 1

HCID 2225361,1-Ethanediol, 1,1-diacetate수율 2,504.6%

시약·촉매·용매 2

HCID 24290Palladium Chloride촉매HCID 176Acetic Acid용매

실험 절차

The procedure of Example 9 was repeated except that 0.451 g of palladium chloride was used in place of palladium supported on activated carbon and the reaction was effected for 3 hours. GC analysis showed that 1.51 g of vinyl acetate and 32.1 g of ethylidene diacetate were formed with considerable amount of acetic acid.

출처 및 근거

ORD 기록
ord-a9b5c18e35584c908a6278b712e5c952
출처 데이터셋
uspto-grants-1990_12
특허 번호
US04978778

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