Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 178495106, 화합물 → HCID 178509798, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 178495106 | HCID 178495106 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | HCID 178509798 | HCID 178509798 | 103% |
반응 단계
A solution of 10.1 g of p-[trans-4-(2-methoxyvinyl)cyclohexyl]benzonitrile in 200 ml of tetrahydrofuran/2N hydrochloric acid (vol. 4:1) was heated to reflux for 1 hour while stirring The reaction mixture was subsequently partitioned three times in diethyl ether/water. The organic extracts were washed twice with water, dried over magnesium sulphate, filtered and evaporated, there being obtained 9.8 g of 2-[trans-4-(p-cyanophenyl)cyclohexyl]acetaldehyde as a light yellowish, crystalline residue.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04980486 |
| 출처 데이터셋 | uspto-grants-1990_12 |
| ORD ID | ord-8c86919976e4458d8198356ddb7ebfb1 |
| 출처 메모 | uspto-grants-1990_12 |