1,10-Decanediamine → N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine]

HRID 1111923노트

반응식

HRID 1111923 반응식
[CH2:1]1[O:7][CH:2]1[CH2:3][CH2:4][CH2:5][CH3:6].[CH2:8]([NH2:19])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][NH2:18]>C(O)(C)C>[CH2:17]([NH:18][CH2:1][CH:2]([OH:7])[CH2:3][CH2:4][CH2:5][CH3:6])[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][NH:19][CH2:1][CH:2]([OH:7])[CH2:3][CH2:4][CH2:5][CH3:6]

참가 물질

4

반응물 2

HCID 13171,10-DecanediamineHCID 150362-Butyloxirane

생성물 1

HCID 21332454N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine]

시약·촉매·용매 1

HCID 3776Isopropanol용매

실험 절차

In a manner similar to that of Example 1, condensation of 1-hexene oxide (34.8 g.) and 1,10-decanediamine (30 g.) and recrystallization of the resulting product from isopropyl alcohol gave N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine] (I: R = CH3 (CH2)3, R' = H, X = (CH2)10, Z = H) (8.9 g., m.p. 127.0°-137.0° C.).

출처 및 근거

ORD 기록
ord-89b84062e24a476d9bc8cee62c315568
출처 데이터셋
uspto-grants-1978_10
특허 번호
US04119668

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