Dimethylformamide → HCID 22765157, 화합물

HRID 1112131노트

반응식

HRID 1112131 반응식
C(N(CC)CC)C.Cl[CH2:9][CH2:10][S:11]([CH2:14][CH2:15][C:16]([NH:18][CH2:19][CH2:20][S:21][CH:22]=[CH2:23])=[O:17])(=[O:13])=[O:12].CN(C)C=[O:27]>>[CH:10]([S:11]([CH2:14][CH2:15][C:16]([NH:18][CH2:19][CH2:20][S:21]([CH:22]=[CH2:23])=[O:27])=[O:17])(=[O:13])=[O:12])=[CH2:9]

참가 물질

4

반응물 3

HCID 6228DimethylformamideHCID 8471TriethylamineHCID 227651493-(2-Chloroethanesulfonyl)-N-[2-(ethenylsulfanyl)ethyl]propanamide

생성물 1

HCID 22765157HCID 22765157, 화합물

실험 절차

0.8 g Triethylamine was added to a solution of 2.0 g Intermediate 2 in 10 ml dimethylformamide. After stirring 1 hour the mixture was filtered and the filtrate evaporated. The residue was recrystallised form ethyl acetate and then from dichloromethanepetrolether. Yield 1.1 g; Mp. 93° C.

후처리

  1. filtrationwas filtered
  2. customthe filtrate evaporated
  3. customThe residue was recrystallised form ethyl acetate

출처 및 근거

ORD 기록
ord-4b5f9f2540a346feb6e9abd33c727aa9
출처 데이터셋
uspto-grants-1978_10
특허 번호
US04120898

반응 노트

불러오는 중…