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Sodium Carbonate → S-[2-(5-Methyl-4-imidazolylmethylthio)ethyl]-N-cyano-N'-methylisothiourea

HRID 1112214
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인쇄 미리보기

반응식

HRID 1112214 반응식
Cl.[CH3:2][C:3]1[NH:7][CH:6]=[N:5][C:4]=1[CH2:8][S:9][CH2:10][CH2:11][S:12][C:13](=[N:17][CH3:18])[NH:14][C:15]#[N:16].C(=O)([O-])[O-].[Na+].[Na+]>>[CH3:2][C:3]1[NH:7][CH:6]=[N:5][C:4]=1[CH2:8][S:9][CH2:10][CH2:11][S:12][C:13](=[N:17][CH3:18])[NH:14][C:15]#[N:16]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

3

반응물 2

HCID 10340Sodium CarbonateHCID 20387431S-[2-(5-methyl-4-imidazolylmethylthio)ethyl]-N-cyano-N'-methylisothiourea hydrochloride

생성물 1

HCID 20387415S-[2-(5-Methyl-4-imidazolylmethylthio)ethyl]-N-cyano-N'-methylisothiourea

실험 절차

This hydrochloride may be treated with aqueous sodium carbonate and the mixture extracted with chloroform and the chloroform extracts evaporated to give the free base.

후처리

  1. extractionthe mixture extracted with chloroform
  2. customthe chloroform extracts evaporated
  3. customto give the free base

출처 및 근거

ORD 기록
ord-2e686f1ded1448ffbdd7d3f2d5849250
출처 데이터셋
uspto-grants-1978_10
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04120966

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