참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Aspirin | HCID 2244 | — |
| 반응물 | Vincamine | HCID 15376 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | Vincamine acetylsalicylate | HCID 86736089 | — |
반응 단계
A solution of 3.6 g (2.10-` moles) of acetylsalicylic acid in 30 mls of ethanol is added to a solution of 7.08 g (2.10-2 moles) of vincamine in 80 mls of ethanol and 60 mls of CHCl3. The mixture is maintained under stirring at 70° C. for 10 minutes and then concentrated to 60 mls. The residue is taken with ethanol (70 mls) and the solvent is evaporated to a final volume of 15 mls.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04122179 |
|---|
| 출처 데이터셋 | uspto-grants-1978_10 |
|---|
| ORD ID | ord-58e56f3178c24e31977211f621595d8e |
|---|
| 출처 메모 | uspto-grants-1978_10 |
|---|
