Hexanoic Acid → Apovincamine caproate

HRID 1112373

반응식

HRID 1112373 반응식
[CH3:1][CH2:2][C@:3]12[CH:19]=[C:18]([C:20]([O:22][CH3:23])=[O:21])[N:17]3[C:9]4=[C:10]([CH2:24][CH2:25][N:7]([C@@H:8]14)[CH2:6][CH2:5][CH2:4]2)[C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=13.[C:26]([OH:33])(=[O:32])[CH2:27][CH2:28][CH2:29][CH2:30][CH3:31]>O>[CH3:1][CH2:2][C@:3]12[CH:19]=[C:18]([C:20]([O:22][CH3:23])=[O:21])[N:17]3[C:9]4=[C:10]([CH2:24][CH2:25][N:7]([C@@H:8]14)[CH2:6][CH2:5][CH2:4]2)[C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=13.[C:26]([O-:33])(=[O:32])[CH2:27][CH2:28][CH2:29][CH2:30][CH3:31]

참가 물질

4

반응물 2

HCID 8892Hexanoic AcidHCID 71204Apovincamine2회

생성물 1

HCID 86736096Apovincamine caproate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

As in the preceding example, from 3.36 g of apovincamine and 1.17 g of caproic acid, there are obtained 4.1 of a semi-solid product, having low melting point, insoluble in water and alcohol, and with an apovincamine content of 71%

출처 및 근거

ORD 기록
ord-0d3c030c8f8e47ab8983e772947a1f27
출처 데이터셋
uspto-grants-1978_10
특허 번호
US04122179

연결된 노트

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