Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → 2,3-dimethoxy N,N-dimethyl 6-hydroxymethyl benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | Meconin | HCID 68437 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2,3-dimethoxy N,N-dimethyl 6-hydroxymethyl benzamide | HCID 22764030 | 100% |
반응 단계
A mixture of 30 g of 6,7-dimethoxy 3H-isobenzofuranone, prepared according to the method described in Example IV, 1 liter of ethanol and 300-400 cm3 of dimethylamine was agitated for several hours and then evaporated under vacuum at 30° - 35° C. The crystallized product was washed with heptane. The 2,3-dimethoxy N,N-dimethyl 6-hydroxymethyl benzamide was obtained in a yield of 100%. F = 90° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04122202 |
| 출처 데이터셋 | uspto-grants-1978_10 |
| ORD ID | ord-873d25c134824e72a3a75654d0a7fb1c |
| 출처 메모 | uspto-grants-1978_10 |