참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hexadecanolide | HCID 7984 | — |
| 반응물 | Diethanolamine | HCID 8113 | — |
| 촉매 | Sodium Methoxide | HCID 10942334 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N,N-bis(2-hydroxyethyl)-16-hydroxyhexadecanamide | HCID 19694613 | 82% |
반응 단계
A 200-ml flask equipped with a stirrer was charged with 16.6 g (158 mmol) of diethanolamine and 20.1 g (79 mmol) of cyclohexadecanolide, to which 0.21 g (3.9 mmol) of sodium methoxide was added. The contents were stirred at 80° C. for 18 hours. After completion of the reaction, water was added, and solids deposited were collected by filtration and recrystallized from methanol, thereby obtaining 23.3 g (yield: 82%) of N,N-bis(2-hydroxyethyl)-16-hydroxyhexadecanamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05723497 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-314181a292b147ec995c4191958340db |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
