Diglyme → HCID 178418794, 화합물

반응식

[CH2:1]([O:3][C:4](=[O:11])[C:5]([N:7](C=O)[NH2:8])=[NH:6])[CH3:2].[CH3:12]OCCOCCOC>>[CH2:1]([O:3][C:4]([C:5]1[N:6]=[CH:12][NH:8][N:7]=1)=[O:11])[CH3:2]

참가 물질

반응물 2

HCID 8150Diglyme

HCID 86590617(N-Formylhydrazino)-imino acetic acid ethyl ester

생성물 1

HCID 178418794HCID 178418794, 화합물수율 85%

실험 절차

A suspension of (N-Formylhydrazino)-imino acetic acid ethyl ester (9.62 g, 60.4 mmol) in diglyme (40 ml) was refluxed for 30 minutes. After cooling, the precipitated crystal was collected by filteration and washed with hexane to give 1H-1,2,4-triazol-3-carboxylic acid ethyl ester (7.28 g). Yield: 85%.

후처리

temperaturewas refluxed for 30 minutes
temperatureAfter cooling
customthe precipitated crystal was collected by filteration
washwashed with hexane

출처 및 근거

ORD 기록: ord-4b7b68e3c87e41339a24a58d40a683c6
출처 데이터셋: uspto-grants-2006_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07098201B2

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