Diglyme → HCID 178418794, 화합물

HRID 11230

반응식

HRID 11230 반응식
[CH2:1]([O:3][C:4](=[O:11])[C:5]([N:7](C=O)[NH2:8])=[NH:6])[CH3:2].[CH3:12]OCCOCCOC>>[CH2:1]([O:3][C:4]([C:5]1[N:6]=[CH:12][NH:8][N:7]=1)=[O:11])[CH3:2]

참가 물질

3

반응물 2

HCID 8150DiglymeHCID 86590617(N-Formylhydrazino)-imino acetic acid ethyl ester

생성물 1

HCID 178418794HCID 178418794, 화합물수율 85%

실험 절차

A suspension of (N-Formylhydrazino)-imino acetic acid ethyl ester (9.62 g, 60.4 mmol) in diglyme (40 ml) was refluxed for 30 minutes. After cooling, the precipitated crystal was collected by filteration and washed with hexane to give 1H-1,2,4-triazol-3-carboxylic acid ethyl ester (7.28 g). Yield: 85%.

후처리

  1. temperaturewas refluxed for 30 minutes
  2. temperatureAfter cooling
  3. customthe precipitated crystal was collected by filteration
  4. washwashed with hexane

출처 및 근거

ORD 기록
ord-4b7b68e3c87e41339a24a58d40a683c6
출처 데이터셋
uspto-grants-2006_08
특허 번호
US07098201B2

연결된 노트

불러오는 중…