Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 4-iodosalicylate → Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-benzyloxy-2-naphthyl]benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 4-iodosalicylate | HCID 11380407 | — |
| 반응물 | 7-(1-Adamantyl)-6-benzyloxy-2-naphthylboronic acid | HCID 22000313 | — |
| 생성물 | Methyl 2-hydroxy-4-[7-(1-adamantyl)-6-benzyloxy-2-naphthyl]benzoate | HCID 22000341 | 36.2% |
반응 단계
Following the basic procedure of Example 7(f), by reacting 5.52 g (13.4 mmol) of 7-(1-adamantyl)-6-benzyloxy-2-naphthylboronic acid with 2.46 g (8.8 mmol) of methyl 2-hydroxy-4-iodobenzoate, 1.65 g (36%) of the expected compound was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05723499 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-0bc171163cc04932b98554480b9c571f |
| 출처 메모 | uspto-grants-1998_03 |