Methyl 4-Iodo-3-methylbenzoate → Methyl 3-methyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)benzoate

참여 물질

역할	이름	HCID	투입량
반응물	Methyl 4-Iodo-3-methylbenzoate	HCID 231757	—
반응물	5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid	HCID 19694676	—
생성물	Methyl 3-methyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)benzoate	HCID 19694687	53%

반응 단계

Following the basic procedure of Example 7(f), by reacting 2.8 g (10 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid with 1.84 g (6.7 mmol) of methyl 3-methyl-4-iodobenzoate, 1.37 g (53%) of methyl 3-methyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)benzoate was obtained in the form of a yellow oil.

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US05723499
출처 데이터셋	uspto-grants-1998_03
ORD ID	ord-7949d567ab7542a8990b7bcf17a467de
출처 메모	uspto-grants-1998_03