참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Methyl bromoacetate | HCID 60984 | — |
| 반응물 | 4-Hydroxy-2-methylindole | HCID 590225 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 2-Methylindol-4-yloxyacetic Acid Methyl Ester | HCID 69130376 | — |
반응 단계
To a solution of 2-methyl-4-hydroxyindole (5 g) in N,N-dimethylformamide (50 ml) was added anhydrous potassium carbonate 11.7 g) and methyl bromoacetate (3.54 ml) at room temperature, and the mixture was stirred at 80° C. for 2 hours. To the reaction solution was added iced water to give the title compound (5.4 g) having the following physical data.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07098234B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_08 |
|---|
| ORD ID | ord-6639fcbb31a44145a65a3054f940eb48 |
|---|
| 출처 메모 | uspto-grants-2006_08 |
|---|
