Benzoic acid, 4-(acetyloxy)- → p-Acetoxybenzoyl chloride

반응식

[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](O)=[O:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].C(Cl)(=O)C([Cl:17])=O>>[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([Cl:17])=[O:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2]

참가 물질

반응물 2

HCID 16865Benzoic acid, 4-(acetyloxy)-

HCID 65578Oxalyl chloride

생성물 1

HCID 2756254p-Acetoxybenzoyl chloride

실험 절차

A mixture of 4-acetoxybenzoic acid (516 mg) and oxalyl chloride (0.5 ml) was stirred for 30 minutes. The mixture was concentrated under reduced pressure to give 4-acetoxybenzoyl chloride.

후처리

concentrationThe mixture was concentrated under reduced pressure

출처 및 근거

ORD 기록: ord-a84bb63544524f4eb4575caeb8371555
출처 데이터셋: uspto-grants-2006_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07098234B2

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