5-Chlorothiophene-2-carbonyl Chloride → HCID 13371095, 화합물

반응식

[N:1]1([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[CH:5]=[CH:4][N:3]=[CH:2]1.[Cl:15][C:16]1[S:20][C:19]([C:21](Cl)=[O:22])=[CH:18][CH:17]=1>>[Cl:15][C:16]1[S:20][C:19]([C:21]([NH:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][N:1]2[CH:5]=[CH:4][N:3]=[CH:2]2)=[O:22])=[CH:18][CH:17]=1

참가 물질

반응물 2

HCID 5892235-Chlorothiophene-2-carbonyl Chloride

HCID 139528611H-Imidazole-1-octanamine

생성물 1

HCID 13371095HCID 13371095, 화합물

실험 절차

When 1H-imidazole-1-octylamine is treated with 5-chlorothiophene-2-carbonyl chloride by the procedure of Example 36, the title compound, m.p. 95°-97° C., was obtained.

출처 및 근거

ORD 기록: ord-9cfb3358c1de4af79845364419f7ca13
출처 데이터셋: uspto-grants-1984_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04489089

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