Sulfuric Acid → Octyl 3-mercaptopropionate

HRID 1154514노트

반응식

HRID 1154514 반응식
C(OC)(=O)C=C.[C:7]([O:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])(=[O:10])[CH:8]=[CH2:9].O[S:21](O)(=O)=O>>[CH2:12]([O:11][C:7](=[O:10])[CH2:8][CH2:9][SH:21])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

참가 물질

4

반응물 3

HCID 1118Sulfuric Acid2회HCID 7294Methyl AcrylateHCID 17258Octyl acrylate

생성물 1

HCID 89128Octyl 3-mercaptopropionate수율 80%

실험 절차

The procedure was as described in Example 1 but in place of methyl acrylate there were employed 184 grams of octyl acrylate and first there were added 250 ml of dilute H2SO4 (4N) and the later 300 ml of dilute H2SO4. After the fractional distillation there were isolated 174.5 grams (corresponding to a yield of 80%) of 3-mercaptopropionic acid octyl ester.

후처리

  1. distillationAfter the fractional distillation there

출처 및 근거

ORD 기록
ord-40168e2812b449e38aa362c27a0deb73
출처 데이터셋
uspto-grants-1984_12
특허 번호
US04490307

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