Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxydiacetyl dichloride → N,N'-Bis-(3-trifluoromethyl-4-nitrophenyl)diglycolamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxydiacetyl dichloride | HCID 88769 | — |
| 반응물 | 4-Nitro-3-(trifluoromethyl)aniline | HCID 94955 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | N,N'-Bis-(3-trifluoromethyl-4-nitrophenyl)diglycolamide | HCID 12790638 | — |
반응 단계
Reflux a mixture of 11.97 g (0.07 mole) of diglycolic acid dichloride and 28.84 g (0.14 mole) of 3-trifluoromethyl-4-nitroaniline in 250 ml of benzene for 1 hour. Isolate the solid product of this example by filtration and obtain analytically pure material by recrystallization from benzene-methanol followed by crystallizatin from pure methanol, mp 137°-138° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04299845 |
| 출처 데이터셋 | uspto-grants-1981_11 |
| ORD ID | ord-722f8a147e1741a69d0d0193a3f7fb08 |
| 출처 메모 | uspto-grants-1981_11 |