Zirconium(IV) propoxide → HCID 86738104, 화합물

HRID 1155179

반응식

HRID 1155179 반응식
C[Si]([O:5][P:6]([CH2:13][CH2:14][CH2:15][C:16]#[N:17])(=[O:12])[O:7][Si](C)(C)C)(C)C.[O-]CCC.[O-]CCC.[O-]CCC.[O-]CCC.[Zr+4:34]>C(Cl)(Cl)(Cl)Cl>[Zr:34].[C:16]([CH2:15][CH2:14][CH2:13][P:6](=[O:5])([O-:12])[O-:7])#[N:17]

참가 물질

4

반응물 2

HCID 90139Zirconium(IV) propoxideHCID 20562954Bistrimethylsilyl-3-cyanopropylphosphonate

생성물 1

HCID 86738104HCID 86738104, 화합물

시약·촉매·용매 1

HCID 5943Carbon Tetrachloride용매

반응 조건

온도
60 °C

실험 절차

A 2.5 ml portion of the above prepared bistrimethylsilyl-3-cyanopropylphosphonate solution in CCl4 was added dropwise 0.049 g of zirconium tetra propoxide. The reaction mixture was heated to 60° C. and filtered. The filtrate was saved. About 0.058 g of zirconium-3-cyanopropylphosphonate was formed.

후처리

  1. filtrationfiltered

출처 및 근거

ORD 기록
ord-d08d503e35b748858bde3cec2426b89d
출처 데이터셋
uspto-grants-1981_11
특허 번호
US04299943

연결된 노트

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