Ethyl propanecarboximidate hydrochloride → HCID 178463245, 화합물

HRID 1155550노트

반응식

HRID 1155550 반응식
[CH2:1]([NH:3][C:4]1[CH:9]=[C:8]([C:10](OCC)(OCC)[CH2:11][NH2:12])[CH:7]=[CH:6][N:5]=1)[CH3:2].Cl.[C:20](=[NH:26])(OCC)[CH2:21][CH3:22]>C(O)C>[CH2:1]([NH:3][C:4]1[CH:9]=[C:8]([C:10]2[N:26]=[C:20]([CH2:21][CH3:22])[NH:12][CH:11]=2)[CH:7]=[CH:6][N:5]=1)[CH3:2]

참가 물질

4

반응물 2

HCID 13000588Ethyl propanecarboximidate hydrochlorideHCID 131452922-(2-Ethylamino-4-pyridyl)-2,2-diethoxyethylamine

생성물 1

HCID 178463245HCID 178463245, 화합물수율 33%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The procedure of Example XB was employed, starting with 2.0 g. (8 mmoles) of 2-(2-ethylamino-4-pyridyl)-2,2-diethoxyethylamine and 1.16 g. (8.3 mmoles) of ethyl propionimidate hydrochloride in 30 ml. of ethanol, to give 605 g. (33%) of the title compound as a white solid, 190°-193° C.

출처 및 근거

ORD 기록
ord-62ade12b9a1d46ce98da697bcae22026
출처 데이터셋
uspto-grants-1981_11
특허 번호
US04302464

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