Hexane → HCID 178511346, 화합물

HRID 1155647

반응식

HRID 1155647 반응식
[NH2:1][CH2:2][CH2:3][NH:4][CH2:5][CH2:6][NH:7][CH2:8][CH2:9][NH:10][CH2:11][CH2:12][NH2:13].C1([CH:20]([CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH3:39])[C:21](O)=[O:22])C=CC=CC=1.[CH3:40][CH2:41][CH2:42][CH2:43][CH2:44][CH3:45]>>[C:42]1([CH2:39][CH2:38][CH2:37][CH2:36][CH2:35][CH2:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:20][C:21]([NH-:1])=[O:22])[CH:41]=[CH:40][CH:45]=[CH:44][CH:43]=1.[C:42]1([CH2:39][CH2:38][CH2:37][CH2:36][CH2:35][CH2:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:20][C:21]([NH-:1])=[O:22])[CH:41]=[CH:40][CH:45]=[CH:44][CH:43]=1.[C:42]1([CH2:39][CH2:38][CH2:37][CH2:36][CH2:35][CH2:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:20][C:21]([NH-:1])=[O:22])[CH:41]=[CH:40][CH:45]=[CH:44][CH:43]=1.[NH2:13][CH2:12][CH2:11][NH:10][CH2:9][CH2:8][NH:7][CH2:6][CH2:5][NH:4][CH2:3][CH2:2][NH2:1]

참가 물질

4

반응물 3

HCID 8058Hexane2회HCID 8197TetraethylenepentamineHCID 220152372-Phenyloctadecanoic acid2회

생성물 1

HCID 178511346HCID 178511346, 화합물

반응 조건

온도
175 °C

실험 절차

Into a 300 ml reaction flask equipped with a thermometer, an agitator and an addition funnel, 6 g (0.03 mole) tetraethylenepentamine was added and heated to 70°-75° C. with agitation. From the addition funnel, 32.4 g (0.09 mole) phenylstearic acid was added over 10 minutes. To insure complete addition of phenylstearic acid, 15-20 ml hexane was added to the addition funnel and thence into the reaction mixture after hexane was allowed to evaporate away, the contents of the flask was placed under reduced pressure and heated to 175° C. with agitation. Heating was continued at 175° C. for 2 hours allowing the condensation water to distill off. The product, tetraethylenepentamine tris(phenylstearoylamide) was viscous, amber colored liquid.

후처리

  1. customInto a 300 ml reaction flask
  2. customequipped with a thermometer
  3. temperatureheated to 70°-75° C. with agitation
  4. customto evaporate away
  5. temperatureHeating
  6. customthe condensation water
  7. distillationto distill off

출처 및 근거

ORD 기록
ord-f8fe0ca93e4d48659534eb6651c3c68e
출처 데이터셋
uspto-grants-1982_06
특허 번호
US04332737

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