Triethylamine → (Methylsulfanyl)methyl 3-methylbutanoate

HRID 1155722노트

반응식

HRID 1155722 반응식
[C:1]([OH:7])(=[O:6])[CH2:2][CH:3]([CH3:5])[CH3:4].[CH3:8][S:9][CH2:10]Cl.C(N(CC)CC)C>>[C:1]([O:7][CH2:8][S:9][CH3:10])(=[O:6])[CH2:2][CH:3]([CH3:5])[CH3:4]

참가 물질

4

반응물 3

HCID 8471TriethylamineHCID 10430Isovaleric AcidHCID 16916Chloromethyl methyl sulfide

생성물 1

HCID 3018316(Methylsulfanyl)methyl 3-methylbutanoate

실험 절차

This product was prepared according to the procedure described in Example 1, by reacting isovaleric acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 78°-79° C./12 mm Hg, nD20 1.4496.

후처리

  1. customThis product was prepared

출처 및 근거

ORD 기록
ord-31a4b19bed464ea5b7e25deb97eed335
출처 데이터셋
uspto-grants-1982_06
특허 번호
US04332829

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