Piperidine, 1-methyl-4-(4-nitrophenoxy)-4-phenyl- → 4-(4-Nitrophenoxy)-4-phenylpiperidine

반응식

C[N:2]1[CH2:7][CH2:6][C:5]([O:14][C:15]2[CH:20]=[CH:19][C:18]([N+:21]([O-:23])=[O:22])=[CH:17][CH:16]=2)([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH2:4][CH2:3]1.C(OC(N1CCC(OC2C=CC([N+]([O-])=O)=CC=2)(C2C=CC=CC=2)CC1)=O)C>>[N+:21]([C:18]1[CH:17]=[CH:16][C:15]([O:14][C:5]2([C:8]3[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=3)[CH2:4][CH2:3][NH:2][CH2:7][CH2:6]2)=[CH:20][CH:19]=1)([O-:23])=[O:22]

참가 물질

반응물 2

HCID 3060390Piperidine, 1-methyl-4-(4-nitrophenoxy)-4-phenyl-

HCID 205365811-Ethoxycarbonyl-4-(4-nitrophenoxy)-4-phenylpiperidine

생성물 1

HCID 200299564-(4-Nitrophenoxy)-4-phenylpiperidine

실험 절차

(oil), from 1-methyl-4-(4-nitrophenoxy)-4-phenylpiperidine, intermediate 1-ethoxycarbonyl-4-(4-nitrophenoxy)-4-phenylpiperidine of m.p. 137° to 138° C.

출처 및 근거

ORD 기록: ord-0a61528d4e1145e39089e61f0cdac5b6
출처 데이터셋: uspto-grants-1982_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04333942

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