Ethyl bromoacetate → Ethyl [6,7-dichloro-1-oxo-2-(p-chlorophenyl)-5-indanyloxy]acetate

HRID 1156187노트

반응식

HRID 1156187 반응식
[Cl:1][C:2]1[C:10]([Cl:11])=[C:9]2[C:5]([CH2:6][CH:7]([C:13]3[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][CH:14]=3)[C:8]2=[O:12])=[CH:4][C:3]=1[OH:20].Br[CH2:22][C:23]([O:25][CH2:26][CH3:27])=[O:24]>>[Cl:1][C:2]1[C:10]([Cl:11])=[C:9]2[C:5]([CH2:6][CH:7]([C:13]3[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][CH:14]=3)[C:8]2=[O:12])=[CH:4][C:3]=1[O:20][CH2:22][C:23]([O:25][CH2:26][CH3:27])=[O:24]

참가 물질

3

반응물 2

HCID 7748Ethyl bromoacetateHCID 130652976,7-Dichloro-5-hydroxy-2-(p-chlorophenyl)-1-indanone

생성물 1

HCID 12774097Ethyl [6,7-dichloro-1-oxo-2-(p-chlorophenyl)-5-indanyloxy]acetate

실험 절차

Reaction of of 6,7-dichloro-5-hydroxy-2-(p-chlorophenyl)-1-indanone with ethyl bromoacetate according to the procedure of Example 1, STEP (a), affords the title compound, m.p. 159.5°-160° (crystallized from ethanol-acetone).

후처리

  1. customaffords
  2. customthe title compound, m.p. 159.5°-160° (crystallized from ethanol-acetone)

출처 및 근거

ORD 기록
ord-a9990990ce474d7496b0dc59e992fedf
출처 데이터셋
uspto-grants-1982_06
특허 번호
US04334088

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