Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → 2,3-Dimethyl-2-aminobutyronitrile hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Potassium Cyanide | HCID 9032 | — |
| 반응물 | 3-Methyl-2-butanone | HCID 11251 | — |
| 반응물 | Ammonium Chloride | HCID 25517 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2,3-Dimethyl-2-aminobutyronitrile hydrochloride | HCID 12945444 | — |
반응 단계
The reactant 2,3-dimethyl-2-aminobutyronitrile hydrochloride was prepared by the following reaction. A solution of 136 grams (g) (2.1 moles) of potassium cyanide in 220 milliliters (ml) of water was added dropwise at 10°-15° C. to a mixture of 172.2 g (2.0 moles) of 3-methyl-2-butanone, 110.2 g (2.1 moles) ammonium chloride, and 300 ml of ether. The mixture was allowed to reach room temperature at which it was stirred overnight.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04335053 |
| 출처 데이터셋 | uspto-grants-1982_06 |
| ORD ID | ord-51f7cd9ddd6e409594d72f31125435f6 |
| 출처 메모 | uspto-grants-1982_06 |