Acrylonitrile → HCID 54377318, 화합물

HRID 1156453노트

반응식

[CH:1]([C:3]1[CH:11]=[CH:10][C:6]([C:7](Cl)=[O:8])=[CH:5][CH:4]=1)=O.[C:12](#[N:15])[CH:13]=C>>[CH:7]([C:6]1[CH:10]=[CH:11][C:3]([CH:1]=[CH:13][C:12]#[N:15])=[CH:4][CH:5]=1)=[O:8]

참가 물질

반응물 2

HCID 7855Acrylonitrile

HCID 124246204-Formylbenzoyl chloride

생성물 1

HCID 54377318HCID 54377318, 화합물수율 44.6%

실험 절차

The procedure described in Example 28 is repeated, except that 8.23 g (0.05 mol) of 4-formylbenzoyl chloride and 3.32 g (0.0625 mol) of acrylonitrile are used. After a reaction time of 3 hours at 120° C., 3.5 g (0.0223 mol) of 4-formylcinnamonitrile are obtained, corresponding to a yield of 44.6% of theory; melting point 122° C. Analysis for C10H7NO (molecular weight 157): calculated C 76.22%, H 4.49%, N 8.91%, found C 76.30%, H 4.55%, N 8.96%.

출처 및 근거

ORD 기록: ord-77e73e27a6294c30b9313798a0d2177d
출처 데이터셋: uspto-grants-1982_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04335054

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