참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | N,N-Diethylacrylamide | HCID 17583 | — |
| 반응물 | 4-Phenylbenzoyl chloride | HCID 84151 | — |
| 생성물 | 4-Phenylcinnamic acid N,N-diethylamide | HCID 54143397 | — |
반응 단계
This compound is prepared from 10.83 g (50 millimols) of biphenyl-4-carboxylic acid chloride and 7.94 g (62.5 millimols) of N,N-diethylacrylamide, the mixture being stirred for 50 minutes at 120° C. The crude product is extracted, in a Soxhlet extractor, with 125 ml of n-hexane, and is recrystallised once from diethyl ether. 8.5 g (15% of theory) of pale yellow crystals, melting point 113.3° C., are obtained. Analysis for C10H21NO: calculated C 81.72%, H 7.53%, N 5.02%; found C 81.44%, H 7.50%, N 4.91%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04335054 |
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| 출처 데이터셋 | uspto-grants-1982_06 |
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| ORD ID | ord-797fb9f8b8ee42a385393deccfc9c292 |
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| 출처 메모 | uspto-grants-1982_06 |
|---|
