3-Methyltetrahydrofuran → 1,3-Dioxolane

HRID 1156492

반응식

HRID 1156492 반응식
ClCC(C)[CH2:4][CH2:5][Cl:6].CC1C[CH2:12][O:11]C1.[Cl:14]CC(C)C(C)CCl.CC1[CH:27](C)[CH2:26][O:25][CH2:24]1>>[Cl:6][CH2:5][CH2:4][O:11][CH2:12][Cl:14].[O:25]1[CH2:26][CH2:27][O:11][CH2:24]1

참가 물질

6

반응물 4

HCID 982303-MethyltetrahydrofuranHCID 5438601,4-Dichloro-2-methylbutaneHCID 5438803,4-DimethyltetrahydrofuranHCID 13561230HCID 13561230, 화합물

생성물 2

HCID 125861,3-DioxolaneHCID 102908101-chloro-2-(chloromethoxy)ethane

실험 절차

Using the reaction procedure described above, dimethyl carbonate is reacted with bis(1-chloro-2-propyl) ether to produce 2,6-dimethyl-p-dioxane, with 1,4-dichloro-2-methylbutane to make 3-methyltetrahydrofuran, with 1,4-dichloro-2,3-dimethylbutane to make 3,4-dimethyltetrahydrofuran, and with chloromethyl 2-chloroethyl ether to produce 1,3-dioxolane.

출처 및 근거

ORD 기록
ord-b2b392aa7c6e4d598c4ff1b5146c3872
출처 데이터셋
uspto-grants-1982_06
특허 번호
US04336195

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