Diphenyl disulfide → HCID 12851837, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:18]3[C:13](=[C:14]([CH3:19])[CH:15]=[CH:16][CH:17]=3)[CH2:12][CH2:11][N:10]=2)=[CH:5][CH:4]=1.C1(SSC2C=CC=CC=2)C=CC=CC=1>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:9]2[C:18]3[C:13](=[C:14]([CH3:19])[CH:15]=[CH:16][CH:17]=3)[CH:12]=[CH:11][N:10]=2)=[CH:7][CH:8]=1

참가 물질

반응물 2

HCID 13436Diphenyl disulfide

HCID 12851823HCID 12851823, 화합물

생성물 1

HCID 12851837HCID 12851837, 화합물

실험 절차

1-(4-Methoxyphenyl)-5-methyl-3,4-dihydroisoquinoline and diphenyl disulfide were reacted in the same way as in step (c) of Example 1 to afford 1-(4-methoxyphenyl)-5-methylisoquinoline as colorless needles having a melting point of 60.4° to 60.8° C.

출처 및 근거

ORD 기록: ord-3ffbec8f0bb6498a95264b02deb2d540
출처 데이터셋: uspto-grants-1982_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04337256

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