HCID 12917743, 화합물 → 2-n-Butyl-5-hydroxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole

HRID 1156967노트

반응식

HRID 1156967 반응식
[CH2:1]([C:5]1[S:6][C:7]2[CH2:13][CH2:12][CH:11]([C:14](OCC)=[O:15])[CH2:10][C:8]=2[N:9]=1)[CH2:2][CH2:3][CH3:4]>CCOCC>[CH2:1]([C:5]1[S:6][C:7]2[CH2:13][CH2:12][CH:11]([CH2:14][OH:15])[CH2:10][C:8]=2[N:9]=1)[CH2:2][CH2:3][CH3:4]

참가 물질

3

반응물 1

HCID 12917743HCID 12917743, 화합물

생성물 1

HCID 129177552-n-Butyl-5-hydroxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole수율 89%

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

The compound is prepared by reduction of the above derivative (III) with AlLiH4 in ether at room temperature. B.p.0.15 =138°-142° C. Yield: 89%.

후처리

  1. customB.p.0.15 =138°-142° C

출처 및 근거

ORD 기록
ord-afa98a571b07408e8cf237274eaf45c9
출처 데이터셋
uspto-grants-1982_06
특허 번호
US04337343

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