Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1'-Biphenyl, 3-nitro- → 3-Aminobiphenyl
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1'-Biphenyl, 3-nitro- | HCID 16450 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-Aminobiphenyl | HCID 16717 | 77.1% |
반응 단계
3-nitrobiphenyl (500 mg, 2.5 mmol) and 10% palladium on carbon (267 mg, 2.5 mmol) were dissolved in methanol (1 mL) and purged with nitrogen and placed under an atmosphere of hydrogen overnight. The reaction mixture was filtered and evaporated to yield 326 mg of the desired amine, which was used directly in Example 12.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07807713B2 |
| 출처 데이터셋 | uspto-grants-2010_10 |
| ORD ID | ord-fb8eac53c5df4318868e93e72310194f |
| 출처 메모 | uspto-grants-2010_10 |