Acetonitrile → (3R)-3-acetamido-3-phenylpropanoic acid
반응식
[C:1]([NH:4][C:5]1([CH2:10][C:11]([OH:13])=[O:12])[CH2:9][CH2:8][CH2:7][CH2:6]1)(=[O:3])[CH3:2].N[C@@H:15](C1C=CC=CC=1)[CH2:16]C(O)=O.CC#N.O.CC#N>O>[C:1]([NH:4][C@@H:5]([C:9]1[CH:8]=[CH:7][CH:6]=[CH:16][CH:15]=1)[CH2:10][C:11]([OH:13])=[O:12])(=[O:3])[CH3:2]참가 물질
6
실험 절차
The title compound is prepared analogously as described for (1-acetylamino-cyclopentyl)-acetic acid from (R)-3-amino-3-phenylpropionic acid. MS (LC-MS): [M+H]+=208.2. tR (HPLC, Waters Symmetry C18 column, 10-95% CH3CN/H2O/3.5 min, 95% CH3CN/H2O, 2 min, CH3CN and H2O containing 0.1% TFA, flow: 0.6 mL/min): 1.16 min.
후처리
- custom1.16 min.
출처 및 근거
- ORD 기록
- ord-fbe8eeb9931246d28a812386c40c8c0f
- 출처 데이터셋
- uspto-grants-2010_10
- 특허 번호
- US07807709B2
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