4-Bromo-1-(phenylsulfonyl)-1H-indole → HCID 67240891, 화합물
반응식
[Br:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][N:6]2[S:11]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)(=[O:13])=[O:12].[CH2:20]([O:27]C1C(Br)=C2C(=CC=1)NC=C2)[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[Br:1][C:2]1[C:10]([O:27][CH2:20][C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][N:6]2[S:11]([C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1)(=[O:13])=[O:12]참가 물질
3
실험 절차
Using the same procedure as for Intermediate 44 starting from 5-(benzyloxy)-4-bromo-1H-indole, 3.85 g (12.7 mmol) yielded 5.71 g (101%) a dark green crystallizing oil. MS (ESI+) for C21H16BrNO3S m/z 442/444 (M+H)+.
후처리
- customyielded 5.71 g (101%) a dark
- customgreen crystallizing oil
출처 및 근거
- ORD 기록
- ord-33d3a0779c9448b4aadd98bdc4d1480d
- 출처 데이터셋
- uspto-grants-2010_10