2',4'-Dihydroxypropiophenone → 1-(3-Chloro-2,4-dihydroxy-phenyl)-propan-1-one

HRID 1161022

반응식

HRID 1161022 반응식
[Cl:1][C:2]1[C:3]([OH:12])=[C:4]([C:9](=[O:11])[CH3:10])[CH:5]=[CH:6][C:7]=1[OH:8].[CH3:13]CC(C1C=CC(O)=CC=1O)=O>>[Cl:1][C:2]1[C:3]([OH:12])=[C:4]([C:9](=[O:11])[CH2:10][CH3:13])[CH:5]=[CH:6][C:7]=1[OH:8]

참가 물질

3

반응물 2

HCID 798562',4'-DihydroxypropiophenoneHCID 57438294HCID 57438294, 화합물

생성물 1

HCID 178422741-(3-Chloro-2,4-dihydroxy-phenyl)-propan-1-one

실험 절차

The title compound was prepared in a similar manner to 1-(3-chloro-2,4-dihydroxy-phenyl)-ethanone (Preparation 3) employing 2,4-dihydroxypropiophenone to give 4.5 g, 37% of an off-white solid. LCMS 1 201 M+.

출처 및 근거

ORD 기록
ord-8c61b041d6bf45c0a518b288c7d97dcd
출처 데이터셋
uspto-grants-2010_10
특허 번호
US07816523B2

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