Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Bromo-2-methylpropane → 5-Bromo-2-isobutoxybenzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Bromo-2-methylpropane | HCID 6555 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 5-Bromo-2-hydroxybenzonitrile | HCID 2757014 | — |
| 촉매 | Tetrabutylammonium Bromide | HCID 74236 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 5-Bromo-2-isobutoxybenzonitrile | HCID 66585134 | — |
반응 단계
5-Bromo-2-hydroxybenzonitrile, isobutyl bromide, and potassium carbonate were heated at 80° C. in DMF in the presence of tetra-n-butylammonium bromide to obtain 5-bromo-2-isobutoxybenzonitrile. F: 254, 256.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07820700B2 |
| 출처 데이터셋 | uspto-grants-2010_10 |
| ORD ID | ord-b4b0ecc83bbf4e49890fadf070de03a2 |
| 출처 메모 | uspto-grants-2010_10 |