Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl Sulfate → Phenyl 2-methoxy-3-methylphenyl ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl Sulfate | HCID 6497 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 6-Phenoxy-o-cresol | HCID 22734681 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Phenyl 2-methoxy-3-methylphenyl ether | HCID 20082997 | 74.8% |
반응 단계
A mixture of 6-phenoxy-o-cresol (7.5 g) and dimethyl sulfate (14 g) and aqueous solution (30 ml) of potassium hydroxide (10.5 g) were treated in a similar manner to that of Example 14-(2). The resultant residue was pulverized with ethanol to give phenyl 2-methoxy-3-methylphenyl ether (6 g). mp 52°-53° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04367238 |
| 출처 데이터셋 | uspto-grants-1983_01 |
| ORD ID | ord-1184ecfe4267478496a28147cca519d9 |
| 출처 메모 | uspto-grants-1983_01 |