참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzoyl Peroxide | HCID 7187 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | 2,3,5,6-Tetrafluorotoluene | HCID 78896 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 3-(Bromomethyl)-1,2,4,5-tetrafluorobenzene | HCID 104377 | — |
반응 단계
A mixture of 2,3,5,6-tetrafluorotoluene (1.7 g), N-bromosuccinimide (1.9 g), dry carbon tetrachloride (10 ml) and benzoyl peroxide (0.01 g) was heated at the reflux temperature for 20 hours, cooled to the ambient temperature (ca.25° C.) filtered and the filtrate diluted with diethyl ether. The ethereal solution was washed with water, dried over anhydrous magnesium sulphate and concentrated by evaporation of the solvents to yield 2,3,5,6-tetrafluorobenzyl bromide as a mobile colourless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04370346 |
|---|
| 출처 데이터셋 | uspto-grants-1983_01 |
|---|
| ORD ID | ord-8fc3a240a9194d0dba4b7b2cf1fd0e24 |
|---|
| 출처 메모 | uspto-grants-1983_01 |
|---|
