Benzyl Bromide → HCID 22218255, 화합물

반응식

[Br:1][C:2]1[C:3]([OH:17])=[CH:4][C:5]2[C:6]([CH3:16])([CH3:15])[CH2:7][CH:8]=[C:9]([CH:12]([CH3:14])[CH3:13])[C:10]=2[CH:11]=1.[CH2:18](Br)[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH2:18]([O:17][C:3]1[CH:4]=[C:5]2[C:10]([C:9]([CH:12]([CH3:13])[CH3:14])=[CH:8][CH2:7][C:6]2([CH3:15])[CH3:16])=[CH:11][C:2]=1[Br:1])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

참가 물질

반응물 2

HCID 7498Benzyl Bromide

HCID 22218215HCID 22218215, 화합물2회

생성물 1

HCID 22218255HCID 22218255, 화합물수율 100%

실험 절차

Following General Procedure O, 3-bromo-5-isopropyl-8,8-dimethyl-7,8-dihydronaphthalen-2-ol (Compound 97, 0.29 g, 0.98 mmol) was reacted with benzylbromide to afford 0.38 g (100%) of the title compound as a yellow oil.

출처 및 근거

ORD 기록: ord-89ac376698f04e608123147da952f2ed
출처 데이터셋: uspto-grants-2003_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06613917B1

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