Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodoethane → 2-Ethyl-5-methylbenzo[b]thiophene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodoethane | HCID 6340 | — |
| 반응물 | 5-Methylbenzo(b)thiophene | HCID 84346 | — |
| 반응물 | HCID 178418306 | HCID 178418306 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-Ethyl-5-methylbenzo[b]thiophene | HCID 595344 | — |
반응 단계
2-ethyl-5-methylbenzo[b]thiophene was prepared in the same manner as described in Example 40A. Reaction of 5-methylbenzo[b]thiophene (3.4 mmoles, 0.50 g), t-BuLi (1.7 m, 5.1 mmoles, 3.0 ml) and ethyl iodide (6.8 mmoles, 0.54 ml) in THF (10 ml) yielded 0.58 g (97%) of a light yellow liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06613804B2 |
| 출처 데이터셋 | uspto-grants-2003_09 |
| ORD ID | ord-384fc3884e1d4a83b98742c0b678d0e5 |
| 출처 메모 | uspto-grants-2003_09 |