Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Chloride → Ethyl 5-(4-benzyl-1-piperazinyl)benzofuran-2-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Chloride | HCID 7503 | — |
| 반응물 | Ethyl 5-(piperazin-1-yl)benzofuran-2-carboxylate | HCID 11266913 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Ethyl 5-(4-benzyl-1-piperazinyl)benzofuran-2-carboxylate | HCID 23508728 | — |
반응 단계
A solution of 1 g of ethyl 5-(1-piperazinyl)-benzofuran-2-carboxylate in 50 ml of dichloromethane is treated with 1 g of benzyl chloride and stirred for 2 hours. After customary working up, ethyl 5-(4-benzyl-1-piperazinyl)benzofuran-2-carboxylate, m.p. 219°-222°, is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05723614 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-9767918db3564609a907b285260c24dc |
| 출처 메모 | uspto-grants-1998_03 |