Carbon Dioxide → HCID 178527662, 화합물

HRID 1172027노트

반응식

HRID 1172027 반응식
[CH2:1]([S:6]([OH:9])(=[O:8])=[O:7])[S:2]([OH:5])(=[O:4])=[O:3].C(=O)([O-])[O-].[Ag+2:14].C(=O)=O>O>[CH2:1]([S:6]([O-:9])(=[O:8])=[O:7])[S:2]([O-:5])(=[O:4])=[O:3].[Ag+2:14]

참가 물질

5

반응물 3

HCID 280Carbon DioxideHCID 10427Methanedisulfonic acidHCID 178418647HCID 178418647, 화합물2회

생성물 1

HCID 178527662HCID 178527662, 화합물

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

A 50% solution of methanedisulfonic acid in water (2.5 grams) was diluted in 25 mL of water into which, while stirring, silver carbonate (3.91 grams) was added slowly. The silver carbonate dissolved with effervescence of carbon dioxide. After the reaction was complete remaining insoluble material was removed by filtration and the filtrate was stripped of water and dried under high vacuum at 45° C. to give 4.9 grams of white crystals.

후처리

  1. customwas removed by filtration
  2. customdried under high vacuum at 45° C.

출처 및 근거

ORD 기록
ord-7bd1a6dd4a404260a7cdcc8cbba5a5f7
출처 데이터셋
uspto-grants-2010_11
특허 번호
US07833693B2

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