Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Vinyltrichlorosilane → HCID 13463725, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Vinyltrichlorosilane | HCID 6413 | — |
| 반응물 | 1,1,1,4,4-Pentachloro-1,4-disilabutane | HCID 101929494 | — |
| 생성물 | HCID 13463725 | HCID 13463725 | — |
반응 단계
Vinyltrichlorosilane (16.8 g, 104 mmol) was heated to 60° C. and 100 μL 10% H2PtCl6/IPA-solution was added. 1,1,1,4,4-pentachloro-1,4-disilabutane (20.4 g, 77.7 mmol) was added slowly during 20 min so that the temperature did not exceed 100° C. The reaction was allowed to proceed for 12 hours at 100° C., after which it was distilled under vacuum at 115-130° C./<1 mbar. The yield was 31.5 g (74.3 mmol, 96%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07833820B2 |
| 출처 데이터셋 | uspto-grants-2010_11 |
| ORD ID | ord-ecc149b50f6746d4a9fec7163b23f264 |
| 출처 메모 | uspto-grants-2010_11 |