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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1172173생성일: 2026년 10월 27일

(6-Methoxy-indan-1-ylidene)-acetic acid ethyl ester → Ethyl (6-methoxyindan-1-yl)acetate

https://huagongshe.com/reaction/1172173

반응식

참여 물질

역할이름HCID투입량
반응물(6-Methoxy-indan-1-ylidene)-acetic acid ethyl esterHCID 67045796—
촉매PalladiumHCID 23938—
용매MethanolHCID 887—
생성물Ethyl (6-methoxyindan-1-yl)acetateHCID 1106434294%

반응 단계

(6-methoxy-indan-1-ylidene)-acetic acid ethyl ester (3.18 g, 14.5 mmol) was dissolved in MeOH (30 ml). A catalytic amount of 10% Pd/C was added and the reaction was stirred under an atmosphere of hydrogen (balloon) for 2 h. The reaction mixture was filtered through Celite to provide pure (6-methoxy-indan-1-yl)-acetic acid ethyl ester (2.98 g, 94%) as a clear oil. LCMS: 235.0 (M+1)+.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07834004B2
출처 데이터셋uspto-grants-2010_11
ORD IDord-5808587534624ece9fe7b05eb901f078
출처 메모uspto-grants-2010_11