Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(6-Methoxy-indan-1-ylidene)-acetic acid ethyl ester → Ethyl (6-methoxyindan-1-yl)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (6-Methoxy-indan-1-ylidene)-acetic acid ethyl ester | HCID 67045796 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Ethyl (6-methoxyindan-1-yl)acetate | HCID 11064342 | 94% |
반응 단계
(6-methoxy-indan-1-ylidene)-acetic acid ethyl ester (3.18 g, 14.5 mmol) was dissolved in MeOH (30 ml). A catalytic amount of 10% Pd/C was added and the reaction was stirred under an atmosphere of hydrogen (balloon) for 2 h. The reaction mixture was filtered through Celite to provide pure (6-methoxy-indan-1-yl)-acetic acid ethyl ester (2.98 g, 94%) as a clear oil. LCMS: 235.0 (M+1)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07834004B2 |
| 출처 데이터셋 | uspto-grants-2010_11 |
| ORD ID | ord-5808587534624ece9fe7b05eb901f078 |
| 출처 메모 | uspto-grants-2010_11 |