돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1172813생성일: 2026년 10월 25일

4-Methoxyphenol → 1-[4-(4-Chlorophenoxy)-2-propylphenyl]-2-(4-methoxyphenoxy)ethanone

https://huagongshe.com/reaction/1172813

반응식

참여 물질

역할이름HCID투입량
반응물4-MethoxyphenolHCID 9015—
반응물Cesium carbonateHCID 10796—
반응물2-Bromo-1-[4-(4-chlorophenoxy)-2-propylphenyl]ethanoneHCID 57420141—
용매DimethylformamideHCID 6228—
용매Ethyl AcetateHCID 8857—
생성물1-[4-(4-Chlorophenoxy)-2-propylphenyl]-2-(4-methoxyphenoxy)ethanoneHCID 68692754—

반응 단계

A mixture of the product from Step 8 (0.50 g, 1.4 mmol), p-methoxyphenol (2.8 mmol) and cesium carbonate (0.91 g, 2.8 mmol) in DMF (10 mL) was stirred at room temperature for 1 h. The reaction mixture was diluted with ethyl acetate and washed with water. The solvent was evaporated and the residue was purified by chromatography on silica gel to give the title product as an oil.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07834036B2
출처 데이터셋uspto-grants-2010_11
ORD IDord-d0b2a8c484c34129829722107e95272c
출처 메모uspto-grants-2010_11