Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1H-imidazole-2-carbaldehyde → 1-(1H-Imidazol-2-ylmethyl)-5-phenoxy-1,2,3,4-tetrahydro-quinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1H-imidazole-2-carbaldehyde | HCID 24955 | — |
| 반응물 | 5-Phenoxy-1,2,3,4-tetrahydroquinoline | HCID 487547 | — |
| 반응물 | Sodium cyanoborohydride | HCID 5003444 | — |
| 촉매 | Zincchloride | HCID 3007855 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 1-(1H-Imidazol-2-ylmethyl)-5-phenoxy-1,2,3,4-tetrahydro-quinoline | HCID 24786231 | — |
반응 단계
Prepared analogously to Example 1, from 5-phenoxy-1,2,3,4-tetrahydro-quinoline, imidazole-2-carboxaldehyde, zinc chloride and sodium cyanoborohydride in methanol. MS (ISP): 306.3 ([M+H]+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07834044B2 |
| 출처 데이터셋 | uspto-grants-2010_11 |
| ORD ID | ord-a086ec077fea473b88ffcff308ab65b2 |
| 출처 메모 | uspto-grants-2010_11 |